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For alkaloid determination, data were collected as positive-ion spectra by means of enhanced mass scan (EMS) over a m/z 100–1,000 Da range at 1,000 Da/s and Enhanced Product Ion (EPI) over a m/z 50–1,000 Da range at 4,000 Da/s

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However, translating animal doses to human equivalents remains imprecise, and the conservative approach favors starting at lower doses and increasing only if needed

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